Stepwise injection potentiometric determination of caffeine in saliva using single-drop microextraction combined with solvent exchange
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منابع مشابه
Single-drop microextraction combined in-line with capillary electrophoresis for the determination of nonsteroidal anti-inflammatory drugs in urine samples.
This study describes a method to determine nonsteroidal anti-inflammatory drugs (NSAIDs) in urine samples based on the use of single-drop microextraction (SDME) in a three-phase design as a preconcentration technique coupled in-line to capillary electrophoresis. Different parameters affecting the extraction efficiency of the SDME process were evaluated (e.g. type of extractant, volume of the mi...
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An in situ single-drop microextraction (SDME) method was developed for trace mercury determination by a miniaturized spectrophotometer, in which a simple and cheap light-emitting diode (LED) was employed as the light source, and a handheld charge coupled device (CCD) was served as the detector. A droplet of 0.006% dithizone-CCl(4) (m/v) was used as extraction phase and hanged on a rolled PTFE t...
متن کاملLow-density solvent-based dispersive liquid-liquid microextraction combined with single-drop microextraction for the fast determination of chlorophenols in environmental water samples by high performance liquid chromatography-ultraviolet detection.
A new format of fast three-phase microextraction by combining low-density solvent-based dispersive liquid-liquid microextraction (DLLME) and single-drop microextraction (SDME) was for the first time developed for the determination of chlorophenols in environmental water samples. The extraction procedure includes a 2 min DLLME pre-extraction and a 10 min SDME back-extraction. A portion of low-de...
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Dispersive Liquid-Liquid MicroExtraction technique based on Solidification of a Floating Organic drop (DLLME-SFO) combined with flame atomic absorption spectrometry was developed for determination of thallium in water sample. An appropriate mixture of acetone and 1-undecanol was rapidly injected into an aqueous sample containing TlCl4- which forms an ion pair with bril...
متن کاملDispersive liquid–liquid microextraction based on solidification of floating organic drop combined with flame atomic absorption spectrometry for determination trace amount of cobalt in water samples
An efficient, rapid, simple, and highly selective dispersive liquid–liquid microextraction basedon solidification of floating organic drop (DLLME-SFOD), combined with flame atomicabsorption spectrometry was developed for preconcentration and determination of trace amountsof cobalt in water samples. In this method, an appropriate mixture of acetone and1-undecanol was injected rapidly into the aq...
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ژورنال
عنوان ژورنال: Talanta
سال: 2016
ISSN: 0039-9140
DOI: 10.1016/j.talanta.2016.01.001